4-Methyl-1H-1,5-benzodiazepin-2(3H)-one

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4-Methyl-2,3-dihydro-1H-1,5-benzodiazepin-2-one monohydrate

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5-Dichloro­acetyl-4-methyl-2,3,4,5-tetra­hydro-1H-1,5-benzodiazepin-2-one hemihydrate

There are two crystallographically independent organic mol-ecules in the asymmetric unit of the title compound, C(12)H(12)Cl(2)N(2)O(2)·0.5H(2)O. The benzodiazepine ring adopts a distorted boat conformation in both molecules. The crystal packing is controlled by N-H⋯O, C-H⋯O and O-H⋯O intra- and inter-molecular hydrogen bonds. A graph-set motif of R(3) (3)(14) dimer formation by a combination o...

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4-Methyl-1-phenyl­quinolin-2(1H)-one

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2-(4-Bromo­phen­yl)-2-methyl-2,3-di­hydro­quinazolin-4(1H)-one

In the title compound, C(15)H(13)BrN(2)O, the pyrimidine ring adopts a skew boat conformation. The amino H atom forms an inter-molecular hydrogen bond with the carbonyl O atom of an adjacent mol-ecule, forming an inversion dimer. Another lone pair of electrons on the same carbonyl O atom acts as acceptor for another N-H⋯O inter-molecular hydrogen bond with a neighbouring mol-ecule, forming chai...

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ژورنال

عنوان ژورنال: IUCrData

سال: 2018

ISSN: 2414-3146

DOI: 10.1107/s2414314618017182